Selegiline hydrochloride synthesis
- Product Name:Selegiline hydrochloride
- CAS Number:14611-52-0
- Molecular formula:C13H18ClN
- Molecular Weight:223.74
3182-95-4
452 suppliers
$5.00/5g
14611-52-0
192 suppliers
$25.00/100mg
Yield:-
Steps:
Multi-step reaction with 5 steps
1.1: sulfuric acid / toluene / 0.5 h / 20 °C
1.2: 20 h / 80 °C
2.1: ammonium hydroxide / 3 h / 30 - 35 °C
3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 5 h / 80 - 85 °C
3.2: 1 h / 25 - 30 °C
4.1: methanol / 3 h / 0 - 10 °C
4.2: 3 h / 0 - 10 °C
4.3: 0 - 10 °C / pH 4-6
5.1: hydrogenchloride / isopropyl alcohol / 2 h / 20 °C
References:
Anhui Baker Bio-pharmaceutical Co., Ltd.;Yue Xiangjun;Wang Zhibang;Tian Lei;Zou Hui;Xu Jingkun;Chen Xiaofeng;Liu Anyou CN110668951, 2020, A
63-91-2
873 suppliers
$10.00/100G
14611-52-0
192 suppliers
$25.00/100mg
73058-30-7
102 suppliers
$115.00/250 mg
14611-52-0
192 suppliers
$25.00/100mg