SORBOHYDROXAMIC ACID synthesis
- Product Name:SORBOHYDROXAMIC ACID
- CAS Number:4076-62-4
- Molecular formula:C6H9NO2
- Molecular Weight:127.14
110-44-1
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$5.00/25g
4076-62-4
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$75.00/100mg
Yield:4076-62-4 72%
Reaction Conditions:
Stage #1: sorbic Acidwith 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide;triethylamine in ethyl acetate;acetonitrile at 20; for 0.5 h;
Stage #2: with hydroxylamine hydroxide in ethyl acetate;acetonitrile at 20;
References:
Ech-Chahad, Abdellah;Minassi, Alberto;Berton, Luca;Appendino, Giovanni [Tetrahedron Letters,2005,vol. 46,# 31,p. 5113 - 5115]