Stannane, tributyl[(phenylmethoxy)methyl]- synthesis
1synthesis methods
- Product Name:Stannane, tributyl[(phenylmethoxy)methyl]-
- CAS Number:66222-28-4
- Molecular formula:C20H36OSn
- Molecular Weight:411.21
Yield:66222-28-4 98%
Reaction Conditions:
in tetrahydrofuran;to a 0°C soln. of Bu3SnLi in THF was added ClCH2OCH2C6H5 (5 min at 0°C), nitrogen or argon atmosphere; vacuum distillation;
References:
Buchwald, Stephen L.;Nielsen, Ralph B.;Dewan, John C. [Organometallics,1989,vol. 8,# 7,p. 1593 - 1598]