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Stibonium, bromotrimethyl-, bromide (9CI) synthesis

1synthesis methods
-

Yield:91002-43-6 45%

Reaction Conditions:

with bromine in tetrachloromethane;

References:

Mente, Donald C.;Mills, Jerry L.;Mitchell, Roy E. [Inorganic Chemistry,1975,vol. 14,# 1,p. 123 - 126] Bamford, C. H.;Levi, D. L.;Newitt, D. M. [Journal of the Chemical Society][Journal of the Chemical Society,1946,p. 468 - 471] Doak, G. O.;Long, G. G.;Key, M. E. [Inorganic Syntheses,1967,vol. 9,p. 92 - 97] Hartmann, H.;Kuehl, G. [Zeitschrift fur Anorganische und Allgemeine Chemie][Zeitschrift fuer Anorganische und Allgemeine Chemie,1961,vol. 312,p. 186 - 194] Hibbert, H. [Berichte der Deutschen Chemischen Gesellschaft,1906,vol. 39,p. 160 - 162] Morgan, G. T.;Davies, G. R. [Proceedings of the Royal Society of London,1926,vol. 110,p. 523 - 534] Schmidbaur, H.;Mitschke, K. H. [Chemische Berichte,1971,vol. 104,p. 1837 - 1841] Wittig, G.;Laib, H. [Liebigs Annalen der Chemie,1953,vol. 580,p. 47 - 68]