t-Butyl peroxylaurate synthesis
2synthesis methods
- Product Name:t-Butyl peroxylaurate
- CAS Number:2123-88-8
- Molecular formula:C16H32O3
- Molecular Weight:272.42
Yield:2123-88-8 60%
Reaction Conditions:
Stage #1: tert.-butylhydroperoxide;lauric acidwith dmap in dichloromethane;water at 0; for 0.166667 h;
Stage #2: with dicyclohexyl-carbodiimide in dichloromethane;water at 0 - 25;
References:
Wei, Dian;Liu, Tu-Ming;Zhou, Bo;Han, Bing [Organic Letters,2020,vol. 22,# 1,p. 234 - 238] Location in patent:supporting information
