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ChemicalBook CAS DataBase List TERT-BUTYL 3-(ETHOXYCARBONYL)-2-OXOPROPYLCARBAMATE

TERT-BUTYL 3-(ETHOXYCARBONYL)-2-OXOPROPYLCARBAMATE synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: triethylamine / tetrahydrofuran / 0.5 h / -30 - -20 °C
2: 1.) diisopropylamine, n-BuLi / 1.) THF, -70 deg C, 30 min, 2.) THF, -65 deg C, 20 min

References:

Kim, Hwa-Ok;Olsen, Richard K.;Choi, Ok-Soon [Journal of Organic Chemistry,1987,vol. 52,# 20,p. 4531 - 4536]