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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
206446-42-6

tert-butyl 3-(pyridin-4-yl)azetidine-1-carboxylate synthesis

7synthesis methods
tert-butyl 3-bromoazetidine-1-carboxylate

1064194-10-0
118 suppliers
$14.00/100mg

1692-15-5 Synthesis
Pyridine-4-boronic acid

1692-15-5
445 suppliers
$6.00/1g

tert-butyl 3-(pyridin-4-yl)azetidine-1-carboxylate

206446-42-6
13 suppliers
inquiry

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Yield:206446-42-6 12%

Reaction Conditions:

with potassium phosphate;tetrakis(triphenylphosphine) palladium(0) in water;N,N-dimethyl-formamide at 60; for 12 h;

References:

WO2021/170046,2021,A1 Location in patent:Paragraph 0239-0241

4-Iodopyridine

15854-87-2
308 suppliers
$6.00/1g

1-Boc-3-iodoazetidine

254454-54-1
254 suppliers
$15.00/1g

tert-butyl 3-(pyridin-4-yl)azetidine-1-carboxylate

206446-42-6
13 suppliers
inquiry

References
4-Iodopyridine

15854-87-2
308 suppliers
$6.00/1g

1-t-Butoxycarbonylazetedin-3-ylzinc iodide, 0.50 M in THF

206446-38-0
7 suppliers
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tert-butyl 3-(pyridin-4-yl)azetidine-1-carboxylate

206446-42-6
13 suppliers
inquiry

References
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
832 suppliers
$13.50/25G

tert-butyl 3-(pyridin-4-yl)azetidine-1-carboxylate

206446-42-6
13 suppliers
inquiry

References
141699-58-3 Synthesis
1-(Tert-butoxycarbonyl)-3-(methanesulfonyloxy)azetidine

141699-58-3
112 suppliers
$6.00/250mg

tert-butyl 3-(pyridin-4-yl)azetidine-1-carboxylate

206446-42-6
13 suppliers
inquiry

References