TERT-BUTYLDIPHENYLPHOSPHINE synthesis
- Product Name:TERT-BUTYLDIPHENYLPHOSPHINE
- CAS Number:6002-34-2
- Molecular formula:C16H19P
- Molecular Weight:242.3
829-85-6
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$33.00/25g
75-65-0
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$10.00/10ml
6002-34-2
107 suppliers
$17.00/250mg
Yield:6002-34-2 92%
Reaction Conditions:
with silica gel in toluene at 100; for 6 h;Inert atmosphere;Temperature;Reagent/catalyst;
Steps:
1-2 Example 2
Under the protection of argon, add 500mL of reaction solvent toluene into the dry reactor, then add 300g of tert-butanol (compound 2), 186g of diphenylphosphine (compound 3), 8.7g of silica, and react at 100 for 6h; After stopping the reaction, the reaction system was cooled to room temperature, extracted, dried, and recrystallized to obtain 222 g of the target product tert-butyldiphenylphosphine (Compound 1) (yield 92%).
References:
CN113105502,2021,A Location in patent:Paragraph 0006; 0014-0017
108-86-1
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677-22-5
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$45.00/10ml
644-97-3
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$14.00/5g
100-58-3
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$18.00/10ml
6002-34-2
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$17.00/250mg
594-19-4
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$27.50/50ml
1079-66-9
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$5.00/5g
6002-34-2
107 suppliers
$17.00/250mg
507-19-7
243 suppliers
$10.00/5g
1079-66-9
423 suppliers
$5.00/5g
6002-34-2
107 suppliers
$17.00/250mg