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ChemicalBook CAS DataBase List Tetra-tert-butyl orthotitanate

Tetra-tert-butyl orthotitanate synthesis

3synthesis methods
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Yield: 84.6%

Reaction Conditions:

with lithium;N,N-dimethyl-formamide in hexanealcohol added at the boil to a suspension of Li in hexane, stirred cooled, TiCl4 and HCON(CH3)2 added dropwise with stirring; upper layer separated, solvent removed, product distilled under vacuum;

References:

Yatluk;Suvorov [Journal of applied chemistry of the USSR,1985,vol. 58,# 8 pt 2,p. 1678 - 1680]

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