Tetraisopropyl Difluoromethylenebisphosphonate synthesis

8synthesis methods

Product Name:Tetraisopropyl Difluoromethylenebisphosphonate
CAS Number:78715-59-0
Molecular formula:C13H28F2O6P2
Molecular Weight:380.3

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Tetraisopropyl Difluoromethylenebisphosphonate

78715-59-0
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Yield:78715-59-0 100%

Reaction Conditions:

Stage #1: Tetraisopropyl methylenediphosphonatewith sodium hexamethyldisilazane in tetrahydrofuran; for 0.0333333 h;
Stage #2: with N-fluorobis(benzenesulfon)imide in tetrahydrofuran;

References:

Boyle, Nicholas A. [Organic Letters,2006,vol. 8,# 2,p. 187 - 189]

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78715-57-8 Synthesis

Tetraisopropyl Fluoromethylenediphosphonate

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References

Phosphonic acid, P-[difluoro(methylthio)methyl]-, bis(1-methylethyl) ester

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681-80-1
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78715-59-0
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1660-95-3
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681-80-1
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78715-57-8 Synthesis

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78715-59-0
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References

75-61-6
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Phosphorous acid, bis(1-methylethyl) ester, sodium salt (1:1)

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References