Tetramethylammonium trifluoromethylselenate synthesis
- Product Name:Tetramethylammonium trifluoromethylselenate
- CAS Number:75264-92-5
- Molecular formula:C9H25F3N2Se
- Molecular Weight:297.2634
373-68-2
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81290-20-2
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75264-92-5
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Yield:75264-92-5 86%
Reaction Conditions:
Stage #1: (trifluoromethyl)trimethylsilanewith red selenium in tetrahydrofuran at -65; for 1 h;Inert atmosphere;
Stage #2: tetramethylammonium fluoride in tetrahydrofuran at 20; for 12 h;Inert atmosphere;Darkness;
References:
Dürr, Alexander B.;Fisher, Henry C.;Kalvet, Indrek;Truong, Khai-Nghi;Schoenebeck, Franziska [Angewandte Chemie - International Edition,2017,vol. 56,# 43,p. 13431 - 13435][Angew. Chem.,2017,vol. 129,# 43,p. 13616 - 13620,5] Location in patent:supporting information
