ChemicalBook CAS DataBase List TEZAMPANEL

TEZAMPANEL synthesis

3synthesis methods

Product Name:TEZAMPANEL
CAS Number:154652-83-2
Molecular formula:C13H21N5O2
Molecular Weight:279.34

Ethyl (3S,4aR,6S,8aR)-6-(hydroxymethyl)-2-(methoxycarbonyl)-1,2,3,4,4a,5,6,7,8,8a-decahydroisoquinoline-3-carboxylate

157006-69-4
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154652-83-2
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) DMSO, oxalyl chloride, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) -78 deg C, 45 min
2: NaH / tetrahydrofuran / 1.) r.t., 30 min, 2.) 0 deg C, 45 min

References:

Ornstein, Paul L.;Augenstein, Nancy K.;Arnold, M. Brian [Journal of Organic Chemistry,1994,vol. 59,# 25,p. 7862 - 7869]

2,3(1H)-Isoquinolinedicarboxylic acid, 6-(2-cyanoethenyl)octahydro-, 3-ethyl 2-methyl ester, [3S-(3α,4aα,6β,8aα)]- (9CI)

160225-05-8
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154652-83-2
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References

67-56-1 Synthesis

67-56-1
740 suppliers
$9.00/25ml

2537-48-6 Synthesis

2537-48-6
323 suppliers
$7.00/10g

157006-69-4
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154652-83-2
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References

TEZAMPANEL Related Search:

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