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ChemicalBook CAS DataBase List THALLIUM (I) ETHOXIDE

THALLIUM (I) ETHOXIDE synthesis

4synthesis methods
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Yield: 80%

Reaction Conditions:

in ethanolTlAc added to soln. of KOEt (prepd. from K and EtOH), suspn. stirred (70°C, 5h), react. mixt. was two layers of liquids; lower layer separated, placed in vac. over P2O5, dried in the dark for 1d, oil filtered through glass filter; elem. anal.;

References:

Neganova, E. G.;Veits, Yu. A.;Byistro, V. K.;Semenenko, N. M.;Borisenko, A. A.;Foss, V. L. [Journal of general chemistry of the USSR,1990,vol. 60,p. 1817 - 1822][J.Gen.Chem.USSR (Engl.Transl.),1990,vol. 60,p. 2036 - 2042]

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