thiane-2-carbonitrile synthesis
- Product Name:thiane-2-carbonitrile
- CAS Number:146428-12-8
- Molecular formula:C6H9NS
- Molecular Weight:127.21
70759-78-3
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: ammonia / methanol / 120 h / Ambient temperature
2: polyphosphoric acid trimethylsilyl ester / benzene / 2 h / Heating
References:
Kataoka, Tadashi;Iwama, Tetsuo;Tsutsumi, Kazuhiro;Nakamura, Yoshihide;Matsumoto, Harutoshi;et al. [Journal of Chemical Research, Miniprint,1992,# 12,p. 3153 - 3194]