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thunberginol A synthesis

9synthesis methods
3-(3,4-Dimethoxyphenyl)-8-methoxy-1H-isochromen-1-one

147666-84-0
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thunberginol A

147666-80-6
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Yield:147666-80-6 98%

Reaction Conditions:

with boron tribromide in dichloromethane at 20; for 2 h;Inert atmosphere;

References:

Tadd, Andrew C.;Fielding, Mark R.;Willis, Michael C. [Chemical Communications,2009,# 44,p. 6744 - 6746] Location in patent:supporting information; experimental part