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317809-68-0

TMSEP synthesis

3synthesis methods
-

Yield:317809-68-0 82%

Reaction Conditions:

Stage #1: trimethylsilylacetylenewith isopropylmagnesium chloride in tetrahydrofuran at 60; for 0.25 h;
Stage #2: 6,13-pentacenequinone in tetrahydrofuran at 60;
Stage #3: with hydrogenchloride;tin(ll) chloride in tetrahydrofuran;water;Further stages.;

References:

Anthony, John E.;Eaton, David L.;Parkin, Sean R. [Organic Letters,2002,vol. 4,# 1,p. 15 - 18]

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