Tosyl-1H-indol-4-amine synthesis

9synthesis methods

Product Name:Tosyl-1H-indol-4-amine
CAS Number:81038-31-5
Molecular formula:C15H14N2O2S
Molecular Weight:286.35

5192-23-4 Synthesis

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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide; paraffin oil / 0.5 h / 20 °C
2.2: 2 h / 20 °C
3.1: hydrogen; palladium 10% on activated carbon / methanol; ethyl acetate / 4 h / 20 °C / 760.05 Torr

References:

Gerwe, Hubert;He, Feng;Pottie, Eline;Stove, Christophe;Decker, Michael [Angewandte Chemie - International Edition,2022,vol. 61,# 26,art. no. E202203034][Angew. Chem.,2022,vol. 134,# 26]

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References

90481-72-4
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References

4H-Indol-4-one, 5-chloro-1,5,6,7-tetrahydro-1-[(4-methylphenyl)sulfonyl]-

95969-07-6
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References

78283-23-5
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References