Tosylethyl-PE2I synthesis
1synthesis methods
- Product Name:Tosylethyl-PE2I
- CAS Number:1391711-43-5
- Molecular formula:C27H32INO5S
- Molecular Weight:609.52
Yield:1391711-43-5 54%
Reaction Conditions:
Stage #1: C18H22INO2with tetra(n-butyl)ammonium hydroxide in water;toluene at 20; for 0.166667 h;
Stage #2: 1,2-bis-tosyloxyethane in acetonitrile at 20; for 2 h;
References:
Stepanov, Vladimir;Krasikova, Raisa;Raus, Liina;Loog, Olavi;Hiltunen, Jukka;Halldin, Christer [Journal of labelled compounds and radiopharmaceuticals,2012,vol. 55,# 6,p. 206 - 210] Location in patent:experimental part