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ChemicalBook CAS DataBase List TRANS-2-TRIDECEN-1-OL

TRANS-2-TRIDECEN-1-OL synthesis

8synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) MeLi*LiBr 2.) DMSO / 1.) 0 deg C, THF, ether, 15 min 2.) from 0 deg C to room temperature, stiring at room temperature 3h
2: 96 percent / DOWEX 50X8 / methanol / 12 h / Ambient temperature
3: 91 percent / LiAlH4 / tetrahydrofuran / 2 h

References:

Chong, J. Michael;Wong, Susanna [Tetrahedron Letters,1986,vol. 27,# 45,p. 5445 - 5448]

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