![](/CAS/GIF/506-42-3.gif)
TRANS-9-OCTADECENOL synthesis
- Product Name:TRANS-9-OCTADECENOL
- CAS Number:506-42-3
- Molecular formula:C18H36O
- Molecular Weight:268.48
![ELAIDIC ACID METHYL ESTER](/CAS/GIF/2462-84-2.gif)
2462-84-2
31 suppliers
$180.00/25mg
![TRANS-9-OCTADECENOL](/CAS/GIF/506-42-3.gif)
506-42-3
56 suppliers
$120.00/100mg
Yield: 98.4%
Reaction Conditions:
with hydrogen in hexane at 200; under 15001.5 Torr; for 8 h;Solvent;
Steps:
5 Active metal Ru modified MeaXbAlc composite catalyst catalyzes the hydrodeoxygenation of fatty acid (ester) to prepare fatty alcohol
General procedure: In a 25 mL reactor,50 mg of oleic acid and 5 mg of each of the 0.3% Ru/MeaXbAlc composite catalysts prepared in Preparation Example 6 shown in Table 1 were added (before use,These composite catalysts were pre-reduced in a closed reactor under a hydrogen atmosphere at room temperature for 3 h)Then add 10 mL of n-hexane,Under a hydrogen atmosphere of 2 MPa,Heated to 200 ° C and under magnetic stirring conditions,Reaction 8h. After the reaction is completed, it is cooled to room temperature.After the exhaust gas is vented, the reaction solution is diluted with n-hexane.Separating the catalyst solids by centrifugation,Thus, a reaction liquid was obtained, and the obtained reaction liquid was subjected to gas chromatography analysis.Gas chromatographic conditions were: GC99 gas chromatography, FID detector, capillary column (HP-5 30m ×0.320mm × 0.25μm), programmed temperature, the initial temperature of the oven is 100 ° C, and the temperature is raised to 160 ° C at a heating rate of 5 ° C / min, and kept3 minutes. The carrier gas was 99.99% high purity nitrogen at a flow rate of 1 mL/min.
References:
University of Science and Technology of China;Zhang Ying;Guo Ziwei;Wang Hao CN109678658, 2019, A Location in patent:Paragraph 0060; 0061; 0062; 0067; 0068; 0082; 0083; 0086
![ELAIDIC ACID](/CAS/GIF/112-79-8.gif)
112-79-8
149 suppliers
$10.00/50mg
![TRANS-9-OCTADECENOL](/CAS/GIF/506-42-3.gif)
506-42-3
56 suppliers
$120.00/100mg
![Methyl Oleate](/CAS/GIF/112-62-9.gif)
112-62-9
467 suppliers
$6.00/25g
![1-Octadecanol](/CAS/GIF/112-92-5.gif)
112-92-5
466 suppliers
$5.00/10g
![Oleyl alcohol](/CAS/GIF/143-28-2.gif)
143-28-2
265 suppliers
$22.00/25mL
![TRANS-9-OCTADECENOL](/CAS/GIF/506-42-3.gif)
506-42-3
56 suppliers
$120.00/100mg
![9-Heptadecenoic acid, methyl ester, (9Z)-](/CAS/20210111/GIF/14101-91-8.gif)
14101-91-8
4 suppliers
inquiry
![Oleyl alcohol](/CAS/GIF/143-28-2.gif)
143-28-2
265 suppliers
$22.00/25mL
![TRANS-9-OCTADECENOL](/CAS/GIF/506-42-3.gif)
506-42-3
56 suppliers
$120.00/100mg
![Oleic acid](/CAS/GIF/112-80-1.gif)
112-80-1
961 suppliers
$5.00/10g
![1-Octadecanol](/CAS/GIF/112-92-5.gif)
112-92-5
466 suppliers
$5.00/10g
![Oleyl alcohol](/CAS/GIF/143-28-2.gif)
143-28-2
265 suppliers
$22.00/25mL
![TRANS-9-OCTADECENOL](/CAS/GIF/506-42-3.gif)
506-42-3
56 suppliers
$120.00/100mg
![ELAIDIC ACID](/CAS/GIF/112-79-8.gif)
112-79-8
149 suppliers
$10.00/50mg
![Stearic acid](/CAS/GIF/57-11-4.gif)
57-11-4
1210 suppliers
$6.00/100g