trans-Bis(triphenylphosphine)palladium dichloride synthesis
- Product Name:trans-Bis(triphenylphosphine)palladium dichloride
- CAS Number:28966-81-6
- Molecular formula:C36H30Cl2P2Pd
- Molecular Weight:701.9
Yield: 99%
Reaction Conditions:
with diethylamine in tetrahydrofuranbyproducts: P(C6H5)3, 1,3-butadiene; Ar, stirred for 24 h at room temp.; volatiles removed, ppt. washed (acetone), solvent removed; NMR;
References:
Hiwatari, Kozo;Kayaki, Yoshihito;Okita, Koshi;Ukai, Tomohiro;Shimizu, Isao;Yamamoto, Akio [Bulletin of the Chemical Society of Japan,2004,vol. 77,# 12,p. 2237 - 2250]
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