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trans,trans-2,8-Decadiene synthesis

4synthesis methods
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Yield:19398-85-7 93 %Spectr.

Reaction Conditions:

with C24H35IrNP;sodium t-butanolate in benzene-d6 at 25; for 10 h;Inert atmosphere;Glovebox;Schlenk technique;stereoselective reaction;

References:

Wang, Yulei;Qin, Chuan;Jia, Xiangqing;Leng, Xuebing;Huang, Zheng [Angewandte Chemie - International Edition,2017,vol. 56,# 6,p. 1614 - 1618][Angew. Chem.,2017,vol. 129,# 6,p. 1636 - 1640] Location in patent:supporting information