TRI-N-BUTYLGERMANIUM CHLORIDE synthesis
- Product Name:TRI-N-BUTYLGERMANIUM CHLORIDE
- CAS Number:2117-36-4
- Molecular formula:C12H27ClGe
- Molecular Weight:279.44
1067-42-1
65 suppliers
$36.00/1g
10038-98-9
109 suppliers
$83.40/5g
2117-36-4
33 suppliers
$28.60/50mg
Yield:2117-36-4 95%
Reaction Conditions:
aluminium trichlorideother Radiation; a mixt. of GeCl4 and tetraalkylgermane in presence of AlCl3 as catalystin a Pyrex tube is irradiated with a light stream of argon for 3 min atatmospheric pressure (microwave irradiation: 300 W) (Ar); identification by (1)H-NMR, gas chromy.;
References:
Laurent, Régis;Laporterie, André;Dubac, Jacques;Berlan, Jacques [Organometallics,1994,vol. 13,# 6,p. 2493 - 2495]