![](/CAS/GIF/1623-19-4.gif)
TRIALLYL PHOSPHATE synthesis
- Product Name:TRIALLYL PHOSPHATE
- CAS Number:1623-19-4
- Molecular formula:C9H15O4P
- Molecular Weight:218.19
![Allyl chloride](/CAS/GIF/107-05-1.gif)
107-05-1
399 suppliers
$16.80/100ML
![TRIALLYL PHOSPHATE](/CAS/GIF/1623-19-4.gif)
1623-19-4
109 suppliers
$85.00/2.5mg
Yield:1623-19-4 152 g
Reaction Conditions:
with aluminum (III) chloride;ammonium dihydrogen phosphate at 30 - 80; for 9 h;Temperature;Reagent/catalyst;
Steps:
1-4 Example 1
To have a reflux condenser,A dry 1000ml three-necked flask with thermometer and exhaust gas absorption device was charged with 229.5g (3mol) of 3-chloropropene,115 g (1 mol) of ammonium dihydrogen phosphate and 2.3 g of anhydrous aluminum trichloride as the catalyst.Under stirring,React at a temperature of 30 to 45°C for 6 hours.There is basically no reflux in the reflux condenser,Then increase the reaction temperature to 70-80°C and continue to keep the temperature for 3 hours.The exhaust gas is absorbed into hydrochloric acid with water.After the reaction, it is cooled to room temperature and filtered.The filtrate is crude triallyl phosphate,Then carry out vacuum distillation,Collect 120130/10mmHg fraction,152 g of triallyl phosphate was obtained,The purity of the product is 99.3%.
References:
Jiangsu Chang Yuanhuasheng New Energies Materials Co., Ltd.;Yang Zhiyong;Li Weifeng;Cao Na;Yang Jianxin;Yin Dengjing;Sun Qiuting CN111825712, 2020, A Location in patent:Paragraph 0038-0052
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107-18-6
2 suppliers
$24.60/100ml
![TRIALLYL PHOSPHATE](/CAS/GIF/1623-19-4.gif)
1623-19-4
109 suppliers
$85.00/2.5mg
![TRIALLYL PHOSPHITE](/CAS/GIF/102-84-1.gif)
102-84-1
53 suppliers
$54.29/10g
![TRIALLYL PHOSPHATE](/CAS/GIF/1623-19-4.gif)
1623-19-4
109 suppliers
$85.00/2.5mg
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7459-72-5
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inquiry
![TRIALLYL PHOSPHATE](/CAS/GIF/1623-19-4.gif)
1623-19-4
109 suppliers
$85.00/2.5mg
![ALLYL IODIDE](/CAS/GIF/556-56-9.gif)
556-56-9
130 suppliers
$10.00/1g
![TRIALLYL PHOSPHATE](/CAS/GIF/1623-19-4.gif)
1623-19-4
109 suppliers
$85.00/2.5mg