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TRIBUTYL(PHENYLETHENYL)TIN synthesis

3synthesis methods
24850-33-7 Synthesis
Allyltributyltin

24850-33-7
183 suppliers
$12.00/5g

80735-94-0 Synthesis
1-PHENYL-3-BUTEN-1-OL

80735-94-0
12 suppliers
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Yield:80735-94-0 71% ,79159-76-5 99%

Reaction Conditions:

Stage #1: allyltributylstanane;benzaldehydewith boron trifluoride diethyl etherate in toluene at -35;Inert atmosphere;
Stage #2: phenylacetylenewith tris(pentafluorophenyl)borate in toluene; for 3 h;Inert atmosphere;Solvent;Temperature;Reagent/catalyst;

References:

Ghosh, Banibrata;Amado-Sierra, Maria Del Rosario I.;Holmes, Daniel;Maleczka, Robert E. [Organic Letters,2014,vol. 16,# 9,p. 2318 - 2321] Location in patent:supporting information