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ChemicalBook CAS DataBase List Tricyclo[3.3.1.13,7]decan-1-ethanesulfonaMide
1283719-69-6

Tricyclo[3.3.1.13,7]decan-1-ethanesulfonaMide synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: sulfuryl dichloride; acetic anhydride / 1,2-dichloro-ethane / 0.5 h / -10 °C / Inert atmosphere
1.2: Inert atmosphere; Cooling with ice
2.1: potassium permanganate / water; acetone / 2 h / 50 °C / Inert atmosphere

References:

Yusuff, Naeem;Dore, Michael;Joud, Carol;Visser, Michael;Springer, Clayton;Xie, Xiaoling;Herlihy, Kara;Porter, Dale;Toure, B. Barry [ACS Medicinal Chemistry Letters,2012,vol. 3,# 7,p. 579 - 583]