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ChemicalBook CAS DataBase List Tridecanal

Tridecanal synthesis

9synthesis methods
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Yield:10486-19-8 100%

Reaction Conditions:

Stage #1: 1-Tridecanolwith oxalyl dichloride;dimethyl sulfoxide in dichloromethane at -60; for 1.5 h;
Stage #2: with triethylamine in dichloromethane at -60; for 0.5 h;

References:

Han, Xiaoyu;Dong, Li;Geng, Caiwei;Jiao, Peng [Organic Letters,2015,vol. 17,# 13,p. 3194 - 3197] Location in patent:supporting information

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