tridecane-1-thiol synthesis
- Product Name:tridecane-1-thiol
- CAS Number:19484-26-5
- Molecular formula:C13H28S
- Molecular Weight:216.43
765-09-3
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Yield:19484-26-5 62%
Reaction Conditions:
Stage #1: 1-bromotridecanewith thiourea in ethanol; for 12 h;Reflux;Inert atmosphere;
Stage #2: with sodium hydroxide in water; for 1 h;Reflux;Inert atmosphere;
References:
Castellano, Sabrina;Milite, Ciro;Feoli, Alessandra;Viviano, Monica;Mai, Antonello;Novellino, Ettore;Tosco, Alessandra;Sbardella, Gianluca [ChemMedChem,2015,vol. 10,# 1,p. 144 - 157] Location in patent:supporting information
