![](/CAS/GIF/2943-75-1.gif)
Triethoxyoctylsilane synthesis
- Product Name:Triethoxyoctylsilane
- CAS Number:2943-75-1
- Molecular formula:C14H32O3Si
- Molecular Weight:276.49
![1-OCTENE](/CAS/GIF/111-66-0.gif)
111-66-0
145 suppliers
$10.00/10ml
![Triethoxysilane](/CAS/GIF/998-30-1.gif)
998-30-1
240 suppliers
$30.00/25g
![Triethoxyoctylsilane](/CAS/GIF/2943-75-1.gif)
2943-75-1
328 suppliers
$8.00/25g
Yield:2943-75-1 100%
Reaction Conditions:
at 90; for 5 h;Inert atmosphere;
Steps:
11 Example 11
In a 500-ml three-necked flask, octene (1.25 mol) was added, and Catalyst 1 (1.25 mmol) prepared in Example 1 was slowly heated to 90°C under a nitrogen atmosphere.While stirring, triethoxyhydrosilane (1.5 mol) was added dropwise through the dropping funnel. The dropwise addition time was 0.5 hours, the reaction temperature was maintained, and the stirring reaction was continued for 5 hours.After cooling to room temperature, the corresponding fractions were collected by distillation under reduced pressure. The conversion of octene was 94.7% as determined by GC-MS.The yield of the β adduct 1-triethoxysilyloctane was 100%.
References:
CN107857776,2018,A Location in patent:Paragraph 0048; 0049
![1-OCTENE](/CAS/GIF/111-66-0.gif)
111-66-0
145 suppliers
$10.00/10ml
![Triethoxysilane](/CAS/GIF/998-30-1.gif)
998-30-1
240 suppliers
$30.00/25g
![Tetraethyl orthosilicate](/CAS/GIF/1978-10-4.gif)
78-10-4
423 suppliers
$12.00/25g
![Triethoxyoctylsilane](/CAS/GIF/2943-75-1.gif)
2943-75-1
328 suppliers
$8.00/25g
![1-OCTENE](/CAS/GIF/111-66-0.gif)
111-66-0
145 suppliers
$10.00/10ml
![Triethoxysilane](/CAS/GIF/998-30-1.gif)
998-30-1
240 suppliers
$30.00/25g
![Tetraethyl orthosilicate](/CAS/GIF/1978-10-4.gif)
78-10-4
423 suppliers
$12.00/25g
![hexaethyl diorthosilicate](/CAS/GIF/2157-42-8.gif)
2157-42-8
6 suppliers
inquiry
![Triethoxyoctylsilane](/CAS/GIF/2943-75-1.gif)
2943-75-1
328 suppliers
$8.00/25g
![1-OCTENE](/CAS/GIF/111-66-0.gif)
111-66-0
145 suppliers
$10.00/10ml
![Triethoxysilane](/CAS/GIF/998-30-1.gif)
998-30-1
240 suppliers
$30.00/25g
![Triethoxyoctylsilane](/CAS/GIF/2943-75-1.gif)
2943-75-1
328 suppliers
$8.00/25g
![Silane, triethoxy-2-octen-1-yl-](/CAS/20210305/GIF/911808-73-6.gif)
911808-73-6
0 suppliers
inquiry
![1-OCTENE](/CAS/GIF/111-66-0.gif)
111-66-0
145 suppliers
$10.00/10ml
![Triethoxysilane](/CAS/GIF/998-30-1.gif)
998-30-1
240 suppliers
$30.00/25g
![N-OCTANE](/CAS/GIF/111-65-9.gif)
111-65-9
241 suppliers
$12.00/25g
![Triethoxyoctylsilane](/CAS/GIF/2943-75-1.gif)
2943-75-1
328 suppliers
$8.00/25g