![](/CAS/GIF/112-27-6.gif)
Triethylene glycol synthesis
- Product Name:Triethylene glycol
- CAS Number:112-27-6
- Molecular formula:C6H14O4
- Molecular Weight:150.17
![ETHYLENE OXIDE](/CAS/GIF/75-21-8.gif)
75-21-8
219 suppliers
$39.10/1mL
![Diethylene glycol](/CAS/GIF/111-46-6.gif)
111-46-6
1058 suppliers
$5.00/25g
![Triethylene glycol](/CAS/GIF/112-27-6.gif)
112-27-6
737 suppliers
$6.00/100g
Yield:-
Reaction Conditions:
with titanium(IV) oxide in tetrahydrofuran at 120; under 2250.23 Torr;Inert atmosphere;
Steps:
2.3. Reaction procedure for alkoxylations with solid catalyst
General procedure: The corresponding nucleophile (water or alcohol, typically 0.5mmol), 1.8 ml of ethylene oxide in THF (6 mmol, 3.3 M) and 65 mg of solid catalyst (25 wt%) were placed in a double-walled 6 mL vial, equipped with a magnetic stirrer. The reactor was closed with a screw cap connected to a manometer. The reactor was purged three times withN2 and finally charged with 3 bars of N2. The reaction mixture wasplaced in a pre-heated oil bath at 120 °C and magnetically stirred over 16 h. At the end of the reaction, the mixture was cooled, filtered,concentrated and analyzed by 1H-NMR and GC-MS.
References:
Ballesteros–Soberanas, Jordi;Leyva–Pérez, Antonio;Martínez–Castelló, Aarón;Oliver–Meseguer, Judit;Tejeda–Serrano, María [Molecular catalysis,2021,vol. 515,art. no. 111927]
![ETHYLENE OXIDE](/CAS/GIF/75-21-8.gif)
75-21-8
219 suppliers
$39.10/1mL
![Ethylene glycol](/CAS/GIF/107-21-1.gif)
107-21-1
1311 suppliers
$10.00/25g
![Diethylene glycol](/CAS/GIF/111-46-6.gif)
111-46-6
1058 suppliers
$5.00/25g
![Triethylene glycol](/CAS/GIF/112-27-6.gif)
112-27-6
737 suppliers
$6.00/100g
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2615-15-8
213 suppliers
$6.00/1g
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64-18-6
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$22.12/250ML
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112-60-7
348 suppliers
$7.00/25g
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4792-15-8
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$6.00/1g
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107-21-1
1311 suppliers
$10.00/25g
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64-19-7
1535 suppliers
$10.00/25ML
![Diethylene glycol](/CAS/GIF/111-46-6.gif)
111-46-6
1058 suppliers
$5.00/25g
![Triethylene glycol](/CAS/GIF/112-27-6.gif)
112-27-6
737 suppliers
$6.00/100g
![ETHYLENE OXIDE](/CAS/GIF/75-21-8.gif)
75-21-8
219 suppliers
$39.10/1mL
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124-38-9
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$214.00/14L
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96-49-1
483 suppliers
$6.00/100g
![Ethylene glycol](/CAS/GIF/107-21-1.gif)
107-21-1
1311 suppliers
$10.00/25g
![Diethylene glycol](/CAS/GIF/111-46-6.gif)
111-46-6
1058 suppliers
$5.00/25g
![Triethylene glycol](/CAS/GIF/112-27-6.gif)
112-27-6
737 suppliers
$6.00/100g
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146669-11-6
7 suppliers
$500.83/5MG
![Triethylene glycol](/CAS/GIF/112-27-6.gif)
112-27-6
737 suppliers
$6.00/100g