Trimethoxy(methylcyclopentadienyl)titanium, 98% synthesis
1synthesis methods
- Product Name:Trimethoxy(methylcyclopentadienyl)titanium, 98%
- CAS Number:706820-38-4
- Molecular formula:C9H16O3Ti
- Molecular Weight:220.0885
Yield:706820-38-4 83%
Reaction Conditions:
with triethylamine in diethyl ether;under Ar; Et2O soln. of MeOH and NEt3 added dropwise at room temp. to Et2O soln. of Ti complex (molar ratio 3:3:1); stirred overnight; filtered; residue washed with Et2O; filtrates combined; solvent removed under vac.; oil distd. at 57-59°C (0.04 mmHg); elem. anal.;
References:
Qian, Xianmiao;Huang, Jiling;Qian, Yanlong [Journal of Organometallic Chemistry,2004,vol. 689,# 9,p. 1503 - 1510]