TRIMETHYLGERMANIUM BROMIDE synthesis
- Product Name:TRIMETHYLGERMANIUM BROMIDE
- CAS Number:1066-37-1
- Molecular formula:C3H9BrGe
- Molecular Weight:197.65
865-52-1
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$44.00/1g
1066-37-1
49 suppliers
$60.00/1g
Yield:1066-37-1 81%
Reaction Conditions:
with bromine;aluminium trichloride in neat (no solvent)Br2 added to Me4Ge contg. catalytic amt. of AlCl3 with stirring, stirred overnight; excess Br2 decolorized by addn. of small amt. of Hg, distd.;
References:
Kozuka, Seizi;Tamura, Shoji;Yamazaki, Tetsuya;Yamaguchi, Shigeru;Tagaki, Waichiro [Bulletin of the Chemical Society of Japan,1985,vol. 58,p. 3277 - 3281]