ChemicalBook CAS DataBase List TRIPHENYLACRYLONITRILE

TRIPHENYLACRYLONITRILE synthesis

6synthesis methods

Product Name:TRIPHENYLACRYLONITRILE
CAS Number:6304-33-2
Molecular formula:C21H15N
Molecular Weight:281.35

1607-57-4 Synthesis

1607-57-4
162 suppliers
$10.00/1g

105-56-6
433 suppliers
$10.00/5ml

6304-33-2
27 suppliers
$58.79/5g

Yield:6304-33-2 81%

Reaction Conditions:

Stage #1: Triphenylvinyl bromidewith copper(I) oxide;oxygen;triphenylphosphine in 1-methyl-pyrrolidin-2-one;Schlenk technique;Sealed tube;
Stage #2: ethyl 2-cyanoacetatewith silver nitrate;acetic acid in 1-methyl-pyrrolidin-2-one at 130; for 18 h;Schlenk technique;Sealed tube;

References:

Wang, Xian-Jin;Zhang, Song-Lin [New Journal of Chemistry,2017,vol. 41,# 24,p. 14826 - 14830] Location in patent:supporting information

119-61-9 Synthesis