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ChemicalBook CAS DataBase List tris(2-methoxyphenyl) phosphate

tris(2-methoxyphenyl) phosphate synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: phosphorus; potassium phosphate; diphenyl diselenide / toluene; dimethyl sulfoxide / 6 h / 60 °C / Schlenk technique; Inert atmosphere
2: dihydrogen peroxide / toluene; dimethyl sulfoxide / 0.5 h / 20 °C / Schlenk technique

References:

Zhang, Yue;Cai, Ziman;Chi, Yangyang;Zeng, Xiangzhe;Chen, Shuanghui;Liu, Yan;Tang, Guo;Zhao, Yufen [Organic Letters,2021,vol. 23,# 13,p. 5158 - 5163]