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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
141196-85-2

troxacitabine synthesis

1synthesis methods
2(1H)-Pyrimidinone, 4-amino-1-[2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-1,3-dioxolan-4-yl]-, (2R-cis)- (9CI)

141119-19-9
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troxacitabine

141196-85-2
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Yield:141196-85-2 79.2%

Reaction Conditions:

with tetrabutyl ammonium fluoride in tetrahydrofuran; for 0.5 h;Ambient temperature;

References:

Kim, Hea O.;Ahn, Soon K.;Alves, Antonio J.;Beach, J. Warren;Jeong, Lak S.;et al [Journal of Medicinal Chemistry,1992,vol. 35,# 11,p. 1987 - 1995]