![](/CAS/20180906/GIF/5090-54-0.gif)
VALERANONE synthesis
- Product Name:VALERANONE
- CAS Number:5090-54-0
- Molecular formula:C15H26O
- Molecular Weight:222.37
![1H-Inden-2-ol,octahydro-1,3a,7a-trimethyl-6-(1-methylethyl)-,(1S,3aR,6R,7aS)-(9CI)](/CAS/GIF/823203-42-5.gif)
823203-42-5
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![VALERANONE](/CAS/20180906/GIF/5090-54-0.gif)
5090-54-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: 76 percent / iodine; triphenylphosphine; imidazole / benzene / 2 h / 20 °C
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dimethylformamide / 0.5 h / 160 °C
2.2: ozone / methanol; CH2Cl2 / -78 °C
2.3: triphenylphosphine / methanol; CH2Cl2 / 8 h / 20 °C
3.1: 76 percent / KOH / tetrahydrofuran; methanol; H2O / 8 h / 20 °C
4.1: 80 percent / H2 / Pd/C / methanol / 12 h / 760 Torr
References:
Srikrishna;Viswajanani;Dinesh [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,2004,vol. 43,# 6,p. 1265 - 1274]
![1(4H)-Naphthalenone, 4a,5,6,7,8,8a-hexahydro-4a,8a-dimethyl-7-(1-methylethyl)-, (4aR,7R,8aR)-](/CAS/20210305/GIF/177533-01-6.gif)
177533-01-6
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![VALERANONE](/CAS/20180906/GIF/5090-54-0.gif)
5090-54-0
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![VALERANONE](/CAS/20180906/GIF/5090-54-0.gif)
5090-54-0
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![VALERANONE](/CAS/20180906/GIF/5090-54-0.gif)
5090-54-0
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![VALERANONE](/CAS/20180906/GIF/5090-54-0.gif)
5090-54-0
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