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ChemicalBook CAS DataBase List Villosin
160598-92-5

Villosin synthesis

7synthesis methods
3243-36-5 Synthesis
Bicyclohomofarnesal

3243-36-5
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Villosin

160598-92-5
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-Bu2BOTf; i-Pr2NEt / CH2Cl2 / -78 °C
1.2: 95 percent / CH2Cl2 / 2 h / -78 °C
2.1: 89 percent / Al2O3 / pyridine / 8 h / Heating

References:

Boukouvalas, John;Wang, Jian-Xin;Marion, Olivier [Tetrahedron Letters,2007,vol. 48,# 44,p. 7747 - 7750]

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