ChemicalBook CAS DataBase List Z-BETA-GLU(OTBU)-OH

Z-BETA-GLU(OTBU)-OH synthesis

9synthesis methods

Product Name:Z-BETA-GLU(OTBU)-OH
CAS Number:83436-45-7
Molecular formula:C17H23NO6
Molecular Weight:337.37

L-Aspartic acid, N-[(phenylmethoxy)carbonyl]-, 1-anhydride with 2-methylpropyl hydrogen carbonate, 4-(1,1-dimethylethyl) ester (9CI)

41446-22-4
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83436-45-7
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: tetrahydrofuran; diethyl ether
2: Et₃N; C₆H₅CO₂Ag
3: 89 percent / aq. LiOH / tetrahydrofuran / 1.5 h / 0 - 20 °C

References:

Raju;Mortell, Kathleen;Anandan, Sampathkumar;O'Dowd, Hardwin;Gao, Hongwu;Gomez, Marcela;Hackbarth, Corinne;Wu, Charlotte;Wang, Wen;Yuan, Zhengyu;White, Richard;Trias, Joaquim;Patel, Dinesh V. [Bioorganic and Medicinal Chemistry Letters,2003,vol. 13,# 14,p. 2413 - 2418]

Pentanedioic acid, 3-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl methyl ester, (3R)- (9CI)

83436-44-6
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83436-45-7
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References

Pentanoic acid, 5-diazo-4-oxo-3-[[(phenylmethoxy)carbonyl]amino]-, 1,1-dimethylethyl ester, (3S)-

118248-02-5
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83436-45-7
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References

5545-52-8 Synthesis

N-Cbz-L-Aspartic acid 4-tert-butyl ester

5545-52-8
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$11.19/1G

83436-45-7
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Pentanedioic acid, 3-[[(phenylmethoxy)carbonyl]amino]-, 1-methyl ester, (3S)-

77856-52-1
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83436-45-7
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References