(Z)-dodec-5-enol synthesis

11synthesis methods

Product Name:(Z)-dodec-5-enol
CAS Number:40642-38-4
Molecular formula:C12H24O
Molecular Weight:184.32

13423-48-8
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) sodiobis(trimethylsilyl)amide / 1.) THF, 50-55 deg C, 2.) -78 deg C; 20 deg C
2: 95 percent / HCl / H₂O; acetone / 20 °C
3: 87 percent / LiAlH₄ / diethyl ether / 20 °C

References:

Kovalev, B. G.;Dzhumakulov, T.;Abduvakhabov, A. A.;Sadykov, A. S. [Doklady Chemistry,1987,vol. 297,# 12,p. 544 - 548][Dokl. Akad. Nauk SSSR Ser. Khim.,1987,vol. 297,# 6,p. 1381 - 1386]

88109-70-0
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40642-38-4
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References

694-54-2 Synthesis

694-54-2
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$16.00/1g

13423-48-8
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References

68820-33-7 Synthesis

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40642-38-4
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References

100-72-1
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$8.00/250mg

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References