ChemicalBook CAS DataBase List Z-GLY-PRO-ALA-OH

Z-GLY-PRO-ALA-OH synthesis

5synthesis methods

Product Name:Z-GLY-PRO-ALA-OH
CAS Number:5891-41-8
Molecular formula:C18H23N3O6
Molecular Weight:377.39

15761-39-4
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5891-41-8
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 1.) isobutylchloroformate, N-methylmorpholine, 2.) N-methylmorpholine / 1.) DMF, -20 deg C, 15 min, 2.) -10 deg C, 30 min
2: 93 percent / CF₃COOH / CH₂Cl₂ / 0.25 h
3: 1.) DCC, 1-hydroxybenzotriazole / 1.) DMF, 0 deg C, 15 min, 2.) DMF, CH₂Cl₂, 0 deg C, 90 min; room temp., 5 h
4: 82 percent / 0.5 N NaOH / methanol / 0.5 h

References:

Dietzgen, Ralf G.;Sander, Evamarie;Christner, Juergen;Jung, Guenther [Zeitschrift fur Naturforschung, B: Chemical Sciences,1987,vol. 42,# 4,p. 441 - 453]

L-Alanine, N-[1-[N-[(phenylmethoxy)carbonyl]glycyl]-L-prolyl]-, methyl ester (9CI)

5891-40-7
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5891-41-8
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References

81110-51-2
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5891-41-8
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References

L-Alanine, 1-[(1,1-dimethylethoxy)carbonyl]-L-prolyl-, methyl ester

36302-04-2
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5891-41-8
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References

L-Proline, 1-[N-[(phenylmethoxy)carbonyl]glycyl]-, pentachlorophenyl ester (9CI)

57294-13-0
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5891-41-8
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References

Z-GLY-PRO-ALA-OH Related Search:

Z-Gly-Pro-βNA BENZYLOXYCARBONYLGLYCYL-L-PROLYL-L-LEUCINE