ZELWYCSDHIFMOP-HAPIZUAHSA-N synthesis

11synthesis methods

Product Name:ZELWYCSDHIFMOP-HAPIZUAHSA-N
CAS Number:59699-82-0
Molecular formula:C22H32O2
Molecular Weight:328.4883

40834-42-2 Synthesis

40834-42-2
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59699-82-0
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Yield:-

Steps:

Multi-step reaction with 9 steps
1: 1.) NaH / 1.) HMPA, 0 deg C, 1 h, 2.) 20 min
2: 1.) ethylmagnesium bromide / 1.) THF, room temperature, 1 h, 2.) 15 min
3: 75 percent / DIBAH / tetrahydrofuran; toluene / 0.5 h / -78 °C
4: 90 percent / H₂ / Lindlar catalyst / methanol / 24 h
5: 80 percent / imidazole / dimethylformamide / 18 h / Ambient temperature
6: 90 percent / LiAlH₄, TiCl₃ / tetrahydrofuran / 0.5 h / Ambient temperature
7: sodium fluoride, pyridinium fluoride / tetrahydrofuran; acetonitrile / 5 h / Ambient temperature
8: MnO₂ / CCl₄ / 0.5 h
9: 60 percent / NaCN, AgO, MnO₂ / 14 h / 40 °C