4-IODOBUTYL ACETATE
- CAS No.
- 40596-44-9
- Chemical Name:
- 4-IODOBUTYL ACETATE
- Synonyms
- 4-IODOBUTYL ACETATE;1-ACETOXY-4-IODOBUTANE;4-iodobutyl acetate 96%;4-ACETOXY-BUTAN-1-IODIDE;4-iodo-1-butanol acetate;1-Butanol, 4-iodo-, 1-acetate;4-Iodobutylacetate, 85%, tech.;4-Iodobutyl acetate, 97%, stab;ACETIC ACID 4-IODO-BUTYL ESTER;4-IODOBUTYL ACETATE, TECH., 85%
- CBNumber:
- CB1210301
- Molecular Formula:
- C6H11IO2
- Molecular Weight:
- 242.05
- MDL Number:
- MFCD00010664
- MOL File:
- 40596-44-9.mol
- MSDS File:
- SDS
Boiling point | 94-95 °C5.5 mm Hg(lit.) |
---|---|
Density | 1.61 g/mL at 25 °C(lit.) |
refractive index |
n |
Flash point | 195 °F |
solubility | Difficult to mix. |
form | liquid |
color | Light green turbid |
Sensitive | Light Sensitive |
CAS DataBase Reference | 40596-44-9(CAS DataBase Reference) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
|||||||||
---|---|---|---|---|---|---|---|---|---|---|
Signal word | Warning | |||||||||
Hazard statements | H227 | |||||||||
Precautionary statements | P210e-P280a-P370+P378a-P403+P235-P501a | |||||||||
Hazard Codes | Xi | |||||||||
Risk Statements | 36/37/38 | |||||||||
Safety Statements | 26-36/37/39 | |||||||||
WGK Germany | 3 | |||||||||
HS Code | 29153900 | |||||||||
NFPA 704 |
|
4-IODOBUTYL ACETATE price More Price(7)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Alfa Aesar | H31826 | 4-Iodobutyl acetate, 96%, stab. with copper | 40596-44-9 | 10g | $63.65 | 2024-03-01 | Buy |
Alfa Aesar | H31826 | 4-Iodobutyl acetate, 96%, stab. with copper | 40596-44-9 | 50g | $196.65 | 2024-03-01 | Buy |
SynQuest Laboratories | 2123-H-02 | 4-Iodobutyl acetate | 40596-44-9 | 50g | $312 | 2021-12-16 | Buy |
SynQuest Laboratories | 2123-H-02 | 4-Iodobutyl acetate | 40596-44-9 | 10g | $141 | 2021-12-16 | Buy |
American Custom Chemicals Corporation | HCH0023951 | 4-IODOBUTYLACETATE 95.00% | 40596-44-9 | 10G | $166.32 | 2021-12-16 | Buy |
4-IODOBUTYL ACETATE Chemical Properties,Uses,Production
Chemical Properties
CLEAR DARK BROWN LIQUID
Uses
4-Iodobutyl acetate is used in the preparation of tricyclohexyl(acetoxybutyl))phosphonium iodide, tri-n-hexyl(acetoxybutyl))phosphonium iodide
Synthesis Reference(s)
Synthetic Communications, 24, p. 951, 1994 DOI: 10.1080/00397919408020770
Synthesis
The synthesis of 4-IODOBUTYL ACETATE is as follows:Acetic acid (0.30mmol, 1.0 equivalent), CuI (0.03mmol, 10.0mol%, 5.7mg) and NaI (0.60mmol, 2.0 equivalent, 89.9mg) were added to a 10mL Schlenk tube equipped with a magnetic stirring device. Vacuum the flask with a pump and backfill it three times with nitrogen. Then, 1.0 mL tetrahydrofuran (12.30 mmol, 41.0 equivalence, 1 mL, c=0.30 M), deionized water (0.45 mmol, 1.5 equivalence) and TMSCF3 (0.36 mmol, 1.2 equivalence) were added under N2 atmosphere. The mixture is stirred at 150°C (thermostatic oil bath pot) for 12 hours. After cooling to room temperature, dilute the mixture with ethyl acetate (15 mL), wash with water and brine, and dry on anhydrousNa2SO4. After Extraction by EtOAc (5 mL x 3), the combined organic layer was dehydrated with anhydrousNa2SO4 and concentrated under reduced pressure. The crude product is purified by rapid chromatography on silica gel to obtain alkyl iodide.
4-IODOBUTYL ACETATE Preparation Products And Raw materials
4-IODOBUTYL ACETATE Suppliers
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Hebei Mojin Biotechnology Co., Ltd | +8613288715578 | sales@hbmojin.com | China | 12470 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | 0551-65418671 | sales@tnjchem.com | China | 34571 | 58 |
Nanjing Triumpharm Co.,Ltd | +86-02586182925 +86-15105172550 | info@triumpharm.com | China | 129 | 58 |
SUZHOU SENFEIDA CHEMICAL CO.,LTD | +86-0512-83500002 +8615195660023 | sales@senfeida.com | China | 5100 | 58 |
Aladdin Scientific | +1-+1(833)-552-7181 | sales@aladdinsci.com | United States | 57511 | 58 |
Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131980 | 58 |
Mainchem Co., Ltd. | +86-0592-6210733 | sale@mainchem.com | China | 32360 | 55 |
Wuhan Aikang Chemical Co., Ltd. | 13002132652 | andriy@akkochemical.com | China | 280 | 58 |
Meryer (Shanghai) Chemical Technology Co., Ltd. | 021-61259108 18621169109 | market03@meryer.com | China | 40240 | 62 |
Alfa Aesar | 400-6106006 | saleschina@alfa-asia.com | China | 30132 | 84 |
View Lastest Price from 4-IODOBUTYL ACETATE manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
---|---|---|---|---|---|---|---|---|
2023-07-28 | 4-IODOBUTYL ACETATE
40596-44-9
|
US $0.00 / KG | 1KG | 99% | 50000KG/month | Hebei Mojin Biotechnology Co., Ltd | ||
2021-08-12 | 4-IODOBUTYL ACETATE
40596-44-9
|
US $15.00-10.00 / KG | 1KG | 99%+ HPLC | Monthly supply of 1 ton | Zhuozhou Wenxi import and Export Co., Ltd |
- 4-IODOBUTYL ACETATE
40596-44-9
- US $0.00 / KG
- 99%
- Hebei Mojin Biotechnology Co., Ltd
- 4-IODOBUTYL ACETATE
40596-44-9
- US $15.00-10.00 / KG
- 99%+ HPLC
- Zhuozhou Wenxi import and Export Co., Ltd
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