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| | Ethyl 6,8-dichlorooctanoate Basic information |
| Product Name: | Ethyl 6,8-dichlorooctanoate | | Synonyms: | 6,8-DICHLOROETHYLOCTANOATE;6,8-Dichlorethylcaprylat;Ethyl-6,8-dichloroctanoate;6,8-Dichloro-octanoic acid ethyl ester;6-HYDROXY-8-CHLOROOCTANOIC ACID ETHYL ESTER ,97+%;ETHYL 6,8-DICHLOROOCTANOATE;6,8-dichloro-octanoicaciethylester;Ethyl 6,8-dichlorooc | | CAS: | 1070-64-0 | | MF: | C10H18Cl2O2 | | MW: | 241.15 | | EINECS: | 435-080-1 | | Product Categories: | 3;1070-64-0 | | Mol File: | 1070-64-0.mol |  |
| | Ethyl 6,8-dichlorooctanoate Chemical Properties |
| Boiling point | 109 °C(Press: 0.7 Torr) | | density | 1.107 g/mL at 25 °C(lit.) | | refractive index | n20/D 1.462(lit.) | | Fp | >230 °F | | storage temp. | Sealed in dry,Room Temperature | | solubility | Chloroform, Ethyl Acetate (Slightly) | | form | Oil | | color | Colourless to Pale Yellow | | CAS DataBase Reference | 1070-64-0(CAS DataBase Reference) |
| | Ethyl 6,8-dichlorooctanoate Usage And Synthesis |
| Chemical Properties | Colourless to Pale Yellow Oil | | Uses | 6,8-Dichlorooctanoic Acid Ethyl Ester is an industrial toxin as well as an intermediate product of lipoic acid synthesis. | | Flammability and Explosibility | Not classified | | Synthesis | Dichloroethane in the organic solvent, 6-hydroxy -Chloro - octanoic acid ethyl ester with chlorinated reagent solid phosgene inN, N-dimethyl benzyl amine for the acid-binding agentEthyl 6-hydroxy-8-chlorooctanoate,Chlorination reagents,N, N-dimethylbenzylamine molar ratio1: 1.05: 0.12,The organic solvent was reacted with 6-hydroxy-8-The weight ratio of ethyl chlorocaprylate was1: 2.4 at a temperature ofN, N-dimethylbenzylamine was added dropwise at 10℃,Insulation temperature of 75 ,Insulation time 150min,In the reaction solution obtained,Water layer, water and 6 - hydroxy -8-chloro-ethyl octanoate weight ratio of 1:3, the upper organic phase.Vacuum distillation to collect vacuum 5mmHg,A temperature of 172-176℃,Ethyl 6,8-dichlorooctanoate,Product mol yield 95.68%, Purity 96.65%The bottom of the liquid base to adjust the pH value of 11,Layered,The upper layer was dewatered with sodium sulfateN, N-dimethylbenzylamine,The molar yield of the product was 96.69%Purity 99.71%.
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| | Ethyl 6,8-dichlorooctanoate Preparation Products And Raw materials |
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