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2-CHLORO-4-(METHYLSULFONYL)ANILINE

2-CHLORO-4-(METHYLSULFONYL)ANILINE structure

CAS No.: 13244-35-4

Chemical Name:: 2-CHLORO-4-(METHYLSULFONYL)ANILINE

Synonyms: 2-CHLORO-4-METHYLSULPHONYLANILINE;TIMTEC-BB SBB003494;LABOTEST-BB LT00441295;2-chloro-4-mesylaniline;2-chloro-4-(methylsulfonyl)-anilin;2-CHLORO-4-(METHYLSULFONYL)ANILINE;4-amino-3-chlorophenylmethylsulfone;4-amino-3-chlorofenylomethylosulfon;4-amino-3-chlorophenylmethylsulphone;2-Chloro-4-methylsulphonylaniline,95%

CBNumber:: CB7160824

Molecular Formula:: C7H8ClNO2S

Molecular Weight:: 205.66

MDL Number:: MFCD00152349

MOL File:: 13244-35-4.mol

MSDS File:: SDS

Last updated:2023-04-27 16:27:43

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2-CHLORO-4-(METHYLSULFONYL)ANILINE Properties

Melting point	191-198 °C
Boiling point	400.1±45.0 °C(Predicted)
Density	1.2326 (rough estimate)
refractive index	1.6000 (estimate)
storage temp.	2-8°C
form	Crystalline Powder
pka	-0.60±0.10(Predicted)
color	Pale purple to gray-brown
CAS DataBase Reference	13244-35-4(CAS DataBase Reference)
EPA Substance Registry System	Benzenamine, 2-chloro-4-(methylsulfonyl)- (13244-35-4)

SAFETY

Risk and Safety Statements

Symbol(GHS)	GHS02
Signal word	Warning
Hazard statements	H226
Precautionary statements	P501-P240-P210-P233-P243-P241-P242-P280-P370+P378-P303+P361+P353-P403+P235
Hazard Codes	Xi
Risk Statements	36/37/38
Safety Statements	37/39-26
Hazard Note	Irritant
HS Code	29309099

2-CHLORO-4-(METHYLSULFONYL)ANILINE price More Price(10)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	S448281	2-CHLORO-4-(METHYLSULFONYL)-ANILINE Aldrich	13244-35-4	50mg	$110	2024-03-01	Buy
AK Scientific	5972AA	2-Chloro-4-(methylsulfonyl)aniline	13244-35-4	1g	$123	2021-12-16	Buy
SynQuest Laboratories	8663-5-01	2-Chloro-4-(methylsulfonyl)aniline	13244-35-4	5G	$149	2021-12-16	Buy
Matrix Scientific	006907	2-Chloro-4-methylsulfonylaniline	13244-35-4	5g	$175	2021-12-16	Buy
SynQuest Laboratories	8663-5-01	2-Chloro-4-(methylsulfonyl)aniline	13244-35-4	25g	$549	2021-12-16	Buy

Product number	Packaging	Price	Buy
S448281	50mg	$110	Buy
5972AA	1g	$123	Buy
8663-5-01	5G	$149	Buy
006907	5g	$175	Buy
8663-5-01	25g	$549	Buy

2-CHLORO-4-(METHYLSULFONYL)ANILINE Chemical Properties,Uses,Production

Chemical Properties

pale purple to grey-brown crystalline powder

Uses

2-Chloro-4-methylsulphonylaniline can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development processes and pharmaceutical and chemical production processes.

Synthesis

A mixture of 2-chloro-4-methylsulfonyl-1- nitro-benzene (4.5 g, 19.10 mmol, 1 eq.) in EtOH (40 mL) and a saturated NH4Cl solution (10 mL) was heated to 90 °C, and then Fe (3.20 g, 57.29 mmol, 3 eq.) was added in one portion. The reaction mixture was stirred at 90 °C for 1 h, after which time TLC analysis (PE:EtOAc = 1:1, Rf(starting material) = 0.7, Rf(product) = 0.31) indicated that the reaction was complete. The reaction was diluted with water (50 mL) and extracted with EtOAc (100 mL x 3). The combined organic layers were washed with water (50 mL x 3) and brine (50 mL x 2), dried over anhydrous sodium sulfate, filtered, and concentrated under reduced pressure. The residue was purified by column chromatography (SiO2, PE:EtOAc = 4:1 to 2:1) to provide 2-chloro-4-methylsulfonyl-aniline (3.7 g, 17.99 mmol, 94.21% yield) as an off-white solid.

2-CHLORO-4-(METHYLSULFONYL)ANILINE synthesis

Synthesis of 2-CHLORO-4-(METHYLSULFONYL)ANILINE from 2-Chloro-4-methylsulfonyl-1-nitrobenzene

2-CHLORO-4-(METHYLSULFONYL)ANILINE Preparation Products And Raw materials

Raw materials

1,2-DICHLORO-4-(METHYLSULFONYL)BENZENE 2-Chloro-4-methylsulfonyl-1-nitrobenzene

Preparation Products

2-CHLORO-4-(METHYLSULFONYL)ANILINE Suppliers

Global( 64)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
Suzhou Victorypharm Co.,Ltd.	+86-13916956214	sales@victory-pharm.com	China	1301	58
Shenzhen Nexconn Pharmatechs Ltd	+86-755-89396905 +86-15013857715	admin@nexconn.com	China	10248	58
Hubei Jusheng Technology Co.,Ltd.	18871490254	linda@hubeijusheng.com	CHINA	28180	58
Alchem Pharmtech,Inc.	8485655694	sales@alchempharmtech.com	United States	63711	58
CONIER CHEM AND PHARMA LIMITED	+8618523575427	sales@conier.com	China	49391	58
Richest Group Ltd	18017061086	oled@richest-group.com	CHINA	5601	58
Career Henan Chemica Co	+86-0371-86658258 15093356674;	laboratory@coreychem.com	China	30255	58
sgtlifesciences pvt ltd	+8617013299288	dj@sgtlifesciences.com	China	12382	58
Hangzhou MolCore BioPharmatech Co.,Ltd.	+86-057181025280; +8617767106207	sales@molcore.com	China	49739	58
Zhengzhou Lingzhiyue Technology Co., Ltd	+86-0371-55074660 +86-13783527580	Lingzhiyue@aliyun.com	China	3144	58

Supplier	Advantage
Suzhou Victorypharm Co.,Ltd.	58
Shenzhen Nexconn Pharmatechs Ltd	58
Hubei Jusheng Technology Co.,Ltd.	58
Alchem Pharmtech,Inc.	58
CONIER CHEM AND PHARMA LIMITED	58
Richest Group Ltd	58
Career Henan Chemica Co	58
sgtlifesciences pvt ltd	58
Hangzhou MolCore BioPharmatech Co.,Ltd.	58
Zhengzhou Lingzhiyue Technology Co., Ltd	58

13244-35-4(2-CHLORO-4-(METHYLSULFONYL)ANILINE)Related Search:

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2-chloro-4-(methylsulfonyl)-anilin 2-chloro-4-(methylsulfonyl)-benzenamin 4-amino-3-chlorofenylomethylosulfon 4-amino-3-chlorophenylmethylsulfone 4-amino-3-chlorophenylmethylsulphone TIMTEC-BB SBB003494 2-CHLORO-4-(METHYLSULFONYL)ANILINE LABOTEST-BB LT00441295 2-CHLORO-4-METHYLSULPHONYLANILINE 95% 2-Chloro-4-methylsulphonylaniline,95% 2-Chloro-4-Methylsulphonylaniline, 95% 2.5GR 2-chloro-4-mesylaniline 2-chloro-4-(methylsulfony)benzenamine Benzenamine, 2-chloro-4-(methylsulfonyl)- 2-CHLORO-4-METHYLSULPHONYLANILINE 13244-35-4 C7H8ClNO2S