6-CHLORO-2-PICOLINIC ACID METHYL ESTER
|
|
6-CHLORO-2-PICOLINIC ACID METHYL ESTER 속성
- 녹는점
- 93-94°
- 끓는 점
- 275.8±20.0 °C(Predicted)
- 밀도
- 1.294±0.06 g/cm3(Predicted)
- 저장 조건
- Keep in dark place,Sealed in dry,Room Temperature
- 산도 계수 (pKa)
- -1.03±0.10(Predicted)
- 물리적 상태
- 고체
- 물리적 상태
- 단단한 모양
- 색상
- 옅은 노랑
- 수용성
- 물에 약간 용해됩니다.
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
| 위험 등급 | IRRITANT | ||
|---|---|---|---|
| HS 번호 | 2933399990 |
6-CHLORO-2-PICOLINIC ACID METHYL ESTER C화학적 특성, 용도, 생산
용도
Methyl 6-chloropyridine-2-carboxylate was coupled with 2-(trimethylstannyl)pyridine to afford methyl 2,2?-bipyridine-6-carboxylate.Synthesis Reference(s)
Synthetic Communications, 14, p. 77, 1984 DOI: 10.1080/00397918408060867Synthesis
6-Chloro-2-picolinic acid methyl ester is prepared by the reaction of methanol and 6-Chloropicolinic acid. The specific synthesis steps are as follows:Add thionyl chloride (3.7 ml, 50.8 mmol) to a solution of 6-chloropicolinic acid (4.0 g, 25.4 mmol) in methanol (85 ml) at 0 C. Stir the resultant solution for 15 minutes at 0 C, 0.5 hours at room temperature, and 6 hours at 50 C. Concentrate the reaction in vacuo and dilute with CHCl3 (150ml). Wash the organic solution with saturated aqueous sodium bicarbonate (3 x 100 ml), and brine (1 x 100 ml) and dry with sodium sulfate. Filtration and concentration afford methyl 6-chloropicolinate 4.38 g (100 percent) as a white solid. 1H NMR (CDCl3): δ 8.05 (m, 1H), 7.73 (m, 1H), 7.42 (m, 1H), 3.95 (s, 3H).
6-CHLORO-2-PICOLINIC ACID METHYL ESTER 준비 용품 및 원자재
원자재
준비 용품
6-CHLORO-2-PICOLINIC ACID METHYL ESTER 공급 업체
글로벌( 213)공급 업체
| 공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
|---|---|---|---|---|---|
| Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 |
info@fdachem.com | China | 19368 | 58 |
| Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 |
sales@capotchem.com | China | 29797 | 60 |
| career henan chemical co | +86-0371-86658258 |
sales@coreychem.com | China | 29914 | 58 |
| Hubei Jusheng Technology Co.,Ltd. | 18871490254 |
linda@hubeijusheng.com | CHINA | 28180 | 58 |
| Accela ChemBio Inc. | (+1)-858-699-3322 |
info@accelachem.com | United States | 19965 | 58 |
| Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 |
sales@chemdad.com | China | 39916 | 58 |
| Alchem Pharmtech,Inc. | 8485655694 |
sales@alchempharmtech.com | United States | 63711 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 |
sales@conier.com | China | 49391 | 58 |
| Fuxin Pharmaceutical | +86-021-021-50872116 +8613122107989 |
contact@fuxinpharm.com | China | 10297 | 58 |
| Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 |
joe@yuhengpharm.com | CHINA | 21149 | 58 |
6-CHLORO-2-PICOLINIC ACID METHYL ESTER 관련 검색:
6-BROMO-4-INDAZOLECARBOXYLIC ACID METHYL ESTER
METHYL 6-OXO-1,6-DIHYDRO-3-PYRIDINECARBOXYLATE
Methyl 6-bromonicotinate
METHYL 6-FORMYLNICOTINATE
methyl 6-chloropyrimidine-4-carboxylate
Methyl 6-bromoisoquinoline-1-carboxylate
Methyl 6-bromohexanoate
Methyl 6-chloronicotinate
METHYL 6-CHLOROPYRIDAZINE-3-CARBOXYLATE
methyl 6-methylpyridine-2-carboxylate
6-BROMOPYRIDINE-2-CARBOXYLIC ACID METHYL ESTER
Methyl 6-bromo-2-naphthoate
6-METHYLPYRAZINE-2-CARBOXYLIC ACID METHYL ESTER
2-Chloro-6-pyrazinecarboxylic acid methyl ester
Methyl 6-HydroxypyriMidine-4-carboxylate
Methyl 6-methylnicotinate
Methyl 3-chloropicolinate
6-Chloropicolinic acid