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ChemicalBook CAS DataBase List 3-BROMO-2-CHLORO-6-PICOLINE

3-BROMO-2-CHLORO-6-PICOLINE synthesis

3synthesis methods
56057-19-3 Synthesis
2-Chloro-3-nitro-6-methylpyridine

56057-19-3
269 suppliers
$7.00/250mg

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 80.5 percent / hydrazine hydrate / Raney nickel / ethanol / 70 deg C, 10 min; room temperature, 0.5 h
2: 60 percent / aq. NaNO2, CuBr, HBr

References:

Ciurla;Puszko [Chemistry of Heterocyclic Compounds,1996,vol. 32,# 10,p. 1173 - 1177]

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