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ChemicalBook CAS DataBase List 4-(4-Iodophenyl)pyridine

4-(4-Iodophenyl)pyridine synthesis

2synthesis methods
-

Yield:83420-59-1 61%

Reaction Conditions:

Stage #1: 4-(pyridin-4-yl)anilinewith tetrafluoroboric acid;sodium nitrite at -10; for 0.5 h;
Stage #2: with potassium iodide in acetone;

References:

Khlobystov, Andrei N.;Brett, Matthew T.;Blake, Alexander J.;Champness, Neil R.;Gill, Peter M. W.;O'Neill, Darragh P.;Teat, Simon J.;Wilson, Claire;Schroeder, Martin [Journal of the American Chemical Society,2003,vol. 125,# 22,p. 6753 - 6761]