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4-(DIMETHYLAMINO)-3-NITROPYRIDINE synthesis

2synthesis methods
1122-58-3 Synthesis
4-Dimethylaminopyridine

1122-58-3
1027 suppliers
$6.00/1g

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Yield: 80%

Reaction Conditions:

Stage #1:dmap with sulfuric acid;nitric acid at 0; for 5 h;
Stage #2: with sodium carbonate

References:

Noritake, Yukinobu;Umezawa, Naoki;Kato, Nobuki;Higuchi, Tsunehiko [Inorganic Chemistry,2013,vol. 52,# 7,p. 3653 - 3662]

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