ChemicalBook CAS DataBase List 4-Hydroxybenzyl cyanide

4-Hydroxybenzyl cyanide synthesis

14synthesis methods

Product Name:4-Hydroxybenzyl cyanide
CAS Number:14191-95-8
Molecular formula:C8H7NO
Molecular Weight:133.15

623-05-2 Synthesis

623-05-2
660 suppliers
$5.00/100mg

109-94-4 Synthesis

109-94-4
464 suppliers
$10.00/10g

14191-95-8
392 suppliers
$6.00/5g

Yield:14191-95-8 94%

Reaction Conditions:

in ethanol

Steps:

2 Preparation of para-hydroxybenzyl cyanide
EXAMPLE 2 Preparation of para-hydroxybenzyl cyanide A mixture of 4.96 g. para-hydroxybenzyl alcohol 2.4 g. sodium cyanide 12 ml. ethanol and 12 ml. ethyl formate is heated with stirring under reflux for a period of ninety minutes. The reaction product is then subjected to the same isolation process as in Example 1 to give a 94% yield of crude product showing a melting point of 58°-61° C. uncorrected.

References:

A. H. Marks & Co., Limited US4378319, 1983, A

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104-47-2 Synthesis