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ChemicalBook CAS DataBase List ALPHA-SEXITHIOPHENE

ALPHA-SEXITHIOPHENE synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: NIS / dimethylformamide / -20 °C
2: 60 percent / KF; basic alumina / PdCl2dppf / 0.08 h / 80 °C / microwave irradiation
3: NBS / dimethylformamide
4: 84 percent / KF; bispinacolatodiboron / PdCl2dppf / toluene; methanol / 0.17 h / 70 °C / microwave irradiation

References:

Melucci;Barbarella;Zambianchi;Di Pietro;Bongini [Journal of Organic Chemistry,2004,vol. 69,# 14,p. 4821 - 4828]

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